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Papers of Lyon Playfair, 1st Baron Playfair of St Andrews, 1795-1910, comprising general correspondence, 1795, 1840-1910, covering a range of subjects relating to Playfair's scientific and political interests, notably with Prince Albert, 1851-[1853], and via Charles Grey, 1850-1861, concerning the Great Exhibition, Alfred, Duke of Edinburgh, 1865-1886, Matthew Arnold, 1883, Sir Charles Barry, 1795-1860, Thomas Francis Bayard, concerning 'Venezuela dispute', 1896, Queen Victoria, 1883, and via Sir Arthur John Bigge, 1895-1898, Charles Booth, 1895, Sir David Brewster, concerning lighthouses,1851-1868, Robert Wilhelm Bunsen, concerning their research, 1841-1849, Edwin Chadwick, concerning agriculture and politics, 1855-1899, concerning pensions, Joseph Chamberlain, concerning the Aged Poor Commission, Venezuela, 1894-1899, Prince Christian of Schleswig-Holstein, concerning the 1851 Commission,1882-1896, Sir Robert Christison, concerning vivisection bill, 1867-1876, Anthony Ashley Cooper, 1852-1874, Charles Darwin, concerning vivisection bill, 1875, Sir Thomas Henry De La Beche, concerning the Geological Survey, 1842-1852, Sir James Dewar, 1885-1898, Albert Edward, Prince of Wales (later Edward VII), 1879-1898, Michael Faraday, 1842-1857, William Ewart Gladstone, 1859-1892, Thomas Graham, 1839-1867, Thomas Henry Huxley, 1854-1891, Henry James, 1898, George Granville Leveson-Gower, [1850]-1889, Justus von Liebig, 1841-1873, Joseph Lister, 1876-1898, David Livingstone, including an account of his exploration in Africa, 1861, John Stuart Mill, 1868, Viscount Horatio Nelson to 'Pollard', 1795, Sir Robert Peel, [1842]-1850, letters of condolence to Lady Playfair on the death of Lord Playfair, 1898.

Family correspondence, comprising letters to various correspondents from Playfair, 1854-1898, notably his son George and daughter-in-law; letters from Edith Playfair (third wife), to her step-son, 1898.

Papers relating to diplomas and appointments, 1840-1892, notably appointment as Professor of Chemistry, Edinburgh University, 1858, Charity Commissioner, 1886, Lord-in-Waiting to Queen Victoria, 1892, Privy Councillor, 1873.

Papers relating to orders and decorations, 1851-1898, notably Order of the Bath, Order of the Legion of Honour and Jubilee Medal.

Records relating to lectures and associated studies organised by Imperial College, 1923-1998, comprising Huxley Memorial Lecture papers, including Committee minutes, 1926-1938; texts of lectures, 1925-1939; correspondence, also relating to the Hofmann and Warington Smyth lectures, 1923-1940; texts of Inaugural lectures, 1955-1997, and correspondence with various professors, 1955-1966; correspondence, 1949-1950, and lecture texts, [1952], for a lecture series 'Ends and Means in Science'; industrial lectures, 1932-1934, 1974; correspondence relating to a lecture on the centenary of H G Wells, 1966; Jubilee lectures, 1977; texts of O'Sullivan lectures, 1984-1989; posters for Memorial Lectures, GEC Lectures, and Science, Technology and Medicine Lectures;
records relating to associated studies, comprising Associated Studies annual reports, 1950-1973; minutes, 1970-1974; correspondence, 1966-1981, including Human Sciences, 1966-1967; Non Technical Studies, 1969-1980; papers relating to Interdisciplinary Studies, 1972; invitations and guides relating to Consort Gallery exhibitions, 1971-1993; correspondence relating to Russian Language classes, 1956-1958; correspondence and minutes of the Art Club, 1953-1970; papers relating to 'Touchstone', 1946-1998, including correspondence and reports, 1946-1956; Centenary Appeal Fund and Touchstone Committee, 1948-1971; Musical Society recitals and concerts, 1950-1998.