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Papers covering Hey's career, 1930-1971, including scientific papers, lectures, notes relating to departmental administration, and papers by others. File of correspondence, 1936-1937, chiefly with Professor William Alexander Waters, Professor of Chemistry at the University of Durham, relating to Waters' investigations into reactions involving free radicals and the subsequent publication of a paper on the same in Chemical Review, and including a draft and final version of Waters' paper on 'Decomposition reactions of the Aromatic Diazo Compounds', read to the Royal Society of Chemistry in Dec 1936.

The collection comprises manuscript notebooks, printed pamphlets, correspondence, a minute book, and photographic and other catalogues, 1768-1970. These notably include notebooks containing descriptions and viewing data relating to astronomical observations carried out at Kew Observatory, Richmond, Surrey, on behalf of King George III, with a printed pamphlet by Nevil Maskelyne, Astronomer Royal, entitled Observations of the transit of Venus over the Sun, 1768-1769; manuscript notebook containing measurements recorded during a test of the accuracy of the H5 chronometer designed by John Harrison, 1772; manuscript notebooks recording daily temperature, barometric, hygrometric and rainfall readings taken at Kew Observatory, Richmond, Surrey, 1773-1840; a printed pamphlet by George Atwood, Fellow of the Royal Society, entitled A Supplement to 'A treatise on the construction and properties of arches' (London, 1804), with manuscript dedication to King George III and related correspondence, 1804-1805; a folio signature book of visits by dignitaries to the George III Museum, 1843-1929; manuscript diary describing the work of the George III Museum including the upkeep of equipment and use of exhibits in experiments, 1850-1880; manuscript minutes of the George III Museum Committee charged with managing the collection, 1880-1885; catalogues relating to the collection, [1841-1970]; correspondence by George Calver, astronomer, relating to telescope design, 1897; series of copper plates and labels advertising the George III Museum, [1841-1926].