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MSS.3259-3285 comprise chiefly scientific material; they include student notebooks on zoology, botany and geology (MSS.3259-3280); scientific logs from the British Antarctic Expedition (MSS.3281-3283), specifically a biological log (MSS.3281-3282) and a log of whales sighted (MS.3283), both spanning 1910-1913; an address delivered in 1913 to the New Zealand branch of the British Medical Association on Mendel's principle of heredity (MS.3284); and some notes on fish and fishing (MS.3285). MSS.5252-5254 comprise more personal and more miscellaneous material. MS.5252 is a scrapbook kept by Lillie, containing news cuttings, photographs and miscellaneous papers, spanning the period c.1845-1910 and including cuttings (with portrait prints) on science and scientists, 1845-1901; caricatures by Lillie of lecturers and staff at Birmingham University, 1904-1905; geological photographs, 1907-1909; family photographs (including a group class portrait at United Services' College, Westward Ho!, c.1892); and ephemera from Cambridge, 1909-1910. MS.5253 comprises cuttings from newspapers and illustrated magazines, spanning 1910-1914 and mainly relating to Robert Falcon Scott's British Antarctic Expedition. Finally MS.5254 comprises correspondence and very miscellaneous papers from the period 1824-1938 (plus some undated material) among them letters to his grandfather John Lillie D.D. (1806-1866), and to his maternal relatives the Macaire family, and letters to Lillie from E.A.N. Arber, Caroline Oates and others.

MSS.3356-3382 comprise journals and memorandum books documenting the various phases of McCormick's career, as follows: MS.3356, sketchbook relating to West Indies and South America voyages, 1824-1825; MS.3357, journal of voyage north of Spitsbergen in the Hecla, 1827; MS.3358, notes of lectures on natural philosophy by Robert Jameson (1774-1854) at Edinburgh University, 1830-1831; MS.3359, diary of voyages to West Indies and South America, 1830-1832; MS.3360, half-pay diaries (7 volumes), 1830-1838; MS.3361, diaries covering 1823-1830, fair copy; MS.3362, sketch book covering voyages in North Sea and West Indies, 1832-1833; MS.3363, diary covering blockade of Dutch coast and voyage to West Indies, 1832-1834; MS.3364, diary of a walking tour in Devon (apparently part of a longer journey of which the other journal volumes are not extant), 1834-1835; MS.3365, diary while fitting out the Antarctic expedition of the Erebus, 1839; MSS.3366-3368, diaries written during the Erebus Antarctic expedition (15 volumes), 1839-1843; MSS.3369-3370, meteorological and ornithological logs respectively of the Erebus Antarctic expedition, 1839-1843; MS.3371, half-pay diaries (4 volumes), 1843-1845; MS.3372, memorandum book on Arctic discovery, chiefly compiled during the voyage of the North Star as part of the search for Sir John Franklin, 1848-1852; MS.3373, diary while fitting out the North Star as part of the search for Sir John Franklin, 1852; MSS.3374-3380, diaries written during the voyage of the North Star as part of the search for Sir John Franklin, 1852-1853; MSS.3381-3382, meteorological tables and sketches respectively, made during the voyage of the North Star as part of the search for Sir John Franklin, 1852-1853. MS.8682 comprises loose miscellaneous material, chiefly printed, relating to various phases of McCormick's career: evolving versions of his Narrative of a Boat-Expedition up the Wellington Channel in the Year 1852 (London: Eyre and Spotteswoode, 1854), plus testimonials, printed items by other authors including the Arctic traveller Dr. Richard King, publisher's advertisements and newspapers.

The collection centres on Wallich's work on biology, particularly marine biology, and his belief that other figures in the field were ignoring or plagiarising his discoveries. As well as his notes, it includes a collection of offprints by Wallich (MS.4969) and a collection of offprints by other scientists, with Wallich's comments (MS.4970).